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- Article] Industrial application of green chromatography-I. Separation and analysis of niacinamide in skincare creams using pure water as the mobile phase
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DocNo of ILP: 2105
Doc. Type: Article
Title: Industrial application of green chromatography-I. Separation and analysis of niacinamide in skincare creams using pure water as the mobile phase
Authors: Yanga, Y; Strickland, Z; Kapalavavi, B; Marple, R; Gamsky, C
Full Name of Authors: Yanga, Yu; Strickland, Zackary; Kapalavavi, Brahmam; Marple, Ronita; Gamsky, Chris
Keywords by Author: Pure water chromatography; High-temperature water chromatography; Subcritical water chromatography; HPLC; Niacin; Niacinamide; 4-Acetamidophenol; Skincare cream; Industrial application; Procter & Gamble
Keywords Plus: TEMPERATURE LIQUID-CHROMATOGRAPHY; FLAME IONIZATION DETECTION; SUBCRITICAL WATER; SUPERHEATED WATER; STATIONARY PHASES; ACID; HPLC; HYDROCARBONS; EXTRACTION; ABSORBENCY
Abstract: In this work, chromatographic separation of niacin and niacinamide using pure water as the sole component in the mobile phase has been investigated. The separation and analysis of niacinamide have been optimized using three columns at different temperatures and various flow rates. Our results clearly demonstrate that separation and analysis of niacinamide from skincare products can be achieved using pure water as the eluent at 60 degrees C on a Waters XTerra MS C18 column, a Waters XBridge C18 column, or at 80 degrees C on a Hamilton PRP-1 column. The separation efficiency, quantification quality, and analysis time of this new method are at least comparable with those of the traditional HPLC methods. Compared with traditional HPLC, the major advantage of this newly developed green chromatography technique is the elimination of organic solvents required in the HPLC mobile phase. In addition, the pure water chromatography separations described in this work can be directly applied in industrial plant settings without further modification of the existing HPLC equipment. (c) 2011 Elsevier B.V. All rights reserved.
Cate of OECD: Chemical sciences
Year of Publication: 2011
Business Area: other
Detail Business: medicine & science
Country: Netherlands
Study Area:
Name of Journal: TALANTA
Language: English
Country of Authors: [Yanga, Yu; Strickland, Zackary; Kapalavavi, Brahmam] E Carolina Univ, Dept Chem, Greenville, NC 27858 USA; [Marple, Ronita; Gamsky, Chris] Procter & Gamble Co, Global Analyt Capabil Org, Cincinnati, OH 45241 USA
Press Adress: Yanga, Y (reprint author), E Carolina Univ, Dept Chem, Greenville, NC 27858 USA.
Email Address: yangy@ecu.edu
Citaion:
Funding: Procter Gamble Company; Golden LEAF Foundation
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Number of Citaion: 35
Publication: ELSEVIER SCIENCE BV
City of Publication: AMSTERDAM
Address of Publication: PO BOX 211, 1000 AE AMSTERDAM, NETHERLANDS
ISSN: 0039-9140
29-Character Source Abbreviation: TALANTA
ISO Source Abbreviation: Talanta
Volume: 84
Version: 1
Start of File: 169
End of File: 174
DOI: 10.1016/j.talanta.2010.12.044
Number of Pages: 6
Web of Science Category: Chemistry, Analytical
Subject Category: Chemistry
Document Delivery Number: 734OC
Unique Article Identifier: WOS:000288342400027
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